| Title |
Solid phase extraction and preconcentration of Cu(II), Pb(II), and Ni(II) in environmental samples on chemically modified Amberlite XAD-4 with a proper Schiff base
|
|---|---|
| Published in |
Environmental Monitoring and Assessment, March 2010
|
| DOI | 10.1007/s10661-010-1417-4 |
| Pubmed ID | |
| Authors |
Berrin Topuz, Mustafa Macit |
| Abstract |
A new chelating resin, Amberlite XAD-4 loaded with N,N-bis(salicylidene)cyclohexanediamine (SCHD), was synthesized and characterized. The resin Amberlite XAD-4-SCHD was used for selective separation, preconcentration, and determination of Cu(II), Pb(II), and Ni(II) ions in water samples by flame atomic absorption spectrometry (FAAS). Effects of pH, concentration, and volume of elution solution; flow rate of elution; and sample solution, sample volume, and interfering ions for the recovery of the analytes were investigated. These metal ions can be desorbed with 0.5-M HNO3 (recovery, 98%-101%). The sorption capacity was found between 1.38×10(-1) and 3.58×10(-1) mmol/g. In order to evaluate the accuracy of the proposed procedure, the certified reference materials, BCR-032 (Moroccan phosphate rock) and BCR-715 (industrial effluent wastewater), were analyzed. The detection limits of the method were found to be 0.11, 1.91, and 0.43 μg/L for Cu(II), Pb(II), and Ni(II), respectively. The method was applied to the extraction and the recovery of copper, lead, and nickel in wastewater and other water samples. |
Mendeley readers
The data shown below were compiled from readership statistics for 18 Mendeley readers of this research output. Click here to see the associated Mendeley record.
Geographical breakdown
| Country | Count | As % |
|---|---|---|
| Unknown | 18 | 100% |
Demographic breakdown
| Readers by professional status | Count | As % |
|---|---|---|
| Student > Ph. D. Student | 4 | 22% |
| Student > Master | 3 | 17% |
| Researcher | 2 | 11% |
| Other | 2 | 11% |
| Student > Doctoral Student | 1 | 6% |
| Other | 4 | 22% |
| Unknown | 2 | 11% |
| Readers by discipline | Count | As % |
|---|---|---|
| Chemistry | 13 | 72% |
| Agricultural and Biological Sciences | 2 | 11% |
| Biochemistry, Genetics and Molecular Biology | 1 | 6% |
| Unknown | 2 | 11% |
Attention Score in Context
This research output has an Altmetric Attention Score of 1. This is our high-level measure of the quality and quantity of online attention that it has received. This Attention Score, as well as the ranking and number of research outputs shown below, was calculated when the research output was last mentioned on 03 August 2014.
All research outputs
#21,358,731
of 23,854,458 outputs
Outputs from Environmental Monitoring and Assessment
#2,266
of 2,748 outputs
Outputs of similar age
#104,273
of 109,027 outputs
Outputs of similar age from Environmental Monitoring and Assessment
#15
of 16 outputs
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