Title |
Validation of a Sulfuric Acid Digestion Method for Inductively Coupled Plasma Mass Spectrometry Quantification of TiO2 Nanoparticles
|
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Published in |
Bulletin of Environmental Contamination and Toxicology, April 2018
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DOI | 10.1007/s00128-018-2336-2 |
Pubmed ID | |
Authors |
Preston S. Watkins, Benjamin T. Castellon, Chiyen Tseng, Moncie V. Wright, Cole W. Matson, George P. Cobb |
Abstract |
A consistent analytical method incorporating sulfuric acid (H2SO4) digestion and ICP-MS quantification has been developed for TiO2 quantification in biotic and abiotic environmentally relevant matrices. Sample digestion in H2SO4 at 110°C provided consistent results without using hydrofluoric acid or microwave digestion. Analysis of seven replicate samples for four matrices on each of 3 days produced Ti recoveries of 97% ± 2.5%, 91 % ± 4.0%, 94% ± 1.8%, and 73 % ± 2.6% (mean ± standard deviation) from water, fish tissue, periphyton, and sediment, respectively. The method demonstrated consistent performance in analysis of water collected over a 1 month. |
X Demographics
Geographical breakdown
Country | Count | As % |
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United Kingdom | 1 | 33% |
Unknown | 2 | 67% |
Demographic breakdown
Type | Count | As % |
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Members of the public | 2 | 67% |
Scientists | 1 | 33% |
Mendeley readers
Geographical breakdown
Country | Count | As % |
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Unknown | 18 | 100% |
Demographic breakdown
Readers by professional status | Count | As % |
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Student > Doctoral Student | 3 | 17% |
Unspecified | 2 | 11% |
Student > Bachelor | 2 | 11% |
Student > Ph. D. Student | 2 | 11% |
Student > Master | 2 | 11% |
Other | 3 | 17% |
Unknown | 4 | 22% |
Readers by discipline | Count | As % |
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Environmental Science | 4 | 22% |
Unspecified | 2 | 11% |
Biochemistry, Genetics and Molecular Biology | 2 | 11% |
Materials Science | 2 | 11% |
Earth and Planetary Sciences | 1 | 6% |
Other | 2 | 11% |
Unknown | 5 | 28% |