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Determination of Trace Elements in Cow Placenta by Tungsten Coil Atomic Emission Spectrometry

Overview of attention for article published in Biological Trace Element Research, January 2017
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Title
Determination of Trace Elements in Cow Placenta by Tungsten Coil Atomic Emission Spectrometry
Published in
Biological Trace Element Research, January 2017
DOI 10.1007/s12011-016-0926-6
Pubmed ID
Authors

Daniel A. Gonçalves, Ana C. Soncin, George L. Donati, Mirian C. dos Santos

Abstract

Tungsten coil atomic emission spectrometry (WCAES) is used to determine trace levels of Mn (403.1 nm) and Cr (425.5 nm) in cow placenta. All samples were collected in Ilha Solteira, SP, Brazil. The instrumental setup is based on a tungsten filament extracted from 150 W, 15 V microscope light bulbs, a solid state power supply, fused silica lens, crossed Czerny-Turner spectrograph, and a thermoelectrically cooled charge-coupled device detector. The limits of detection (LOD) and quantification (LOQ) for Cr are 2 and 8 μg L(-1), and 20 and 60 μg L(-1) for Mn, respectively. Recoveries for 0.30 mg L(-1) spikes of each analyte were in the range 93.0-103.0%, and relative standard deviation (RSD) was between 6.50 and 7.20% for both elements. Placenta samples were microwave-assisted digested with diluted HNO3 and H2O2 and analyzed by WCAES. The results for Cr and Mn were compared with values obtained by tandem inductively coupled plasma mass spectrometry (ICP-MS/MS). No statistically significant difference was observed between the different methods by applying a paired t test at a 95% confidence level. The average concentrations of Cr and Mn in the placentas evaluated were 0.95 ± 0.22 and 2.64 ± 0.39 μg g(-1), respectively. By using a short integration time, LODs for Cr and Mn were lower than values reported by recent works using a similar WCAES system.

Mendeley readers

Mendeley readers

The data shown below were compiled from readership statistics for 11 Mendeley readers of this research output. Click here to see the associated Mendeley record.

Geographical breakdown

Country Count As %
Unknown 11 100%

Demographic breakdown

Readers by professional status Count As %
Student > Master 2 18%
Professor 2 18%
Student > Bachelor 1 9%
Student > Ph. D. Student 1 9%
Professor > Associate Professor 1 9%
Other 0 0%
Unknown 4 36%
Readers by discipline Count As %
Chemistry 3 27%
Business, Management and Accounting 1 9%
Agricultural and Biological Sciences 1 9%
Nursing and Health Professions 1 9%
Medicine and Dentistry 1 9%
Other 1 9%
Unknown 3 27%
Attention Score in Context

Attention Score in Context

This research output has an Altmetric Attention Score of 1. This is our high-level measure of the quality and quantity of online attention that it has received. This Attention Score, as well as the ranking and number of research outputs shown below, was calculated when the research output was last mentioned on 11 July 2017.
All research outputs
#15,469,838
of 22,988,380 outputs
Outputs from Biological Trace Element Research
#1,081
of 2,044 outputs
Outputs of similar age
#256,210
of 419,052 outputs
Outputs of similar age from Biological Trace Element Research
#11
of 24 outputs
Altmetric has tracked 22,988,380 research outputs across all sources so far. This one is in the 22nd percentile – i.e., 22% of other outputs scored the same or lower than it.
So far Altmetric has tracked 2,044 research outputs from this source. They receive a mean Attention Score of 4.7. This one is in the 38th percentile – i.e., 38% of its peers scored the same or lower than it.
Older research outputs will score higher simply because they've had more time to accumulate mentions. To account for age we can compare this Altmetric Attention Score to the 419,052 tracked outputs that were published within six weeks on either side of this one in any source. This one is in the 30th percentile – i.e., 30% of its contemporaries scored the same or lower than it.
We're also able to compare this research output to 24 others from the same source and published within six weeks on either side of this one. This one is in the 41st percentile – i.e., 41% of its contemporaries scored the same or lower than it.